Good Laboratory Practice

BRUKER BIOSPIN GMBH, NMR-DEPARTMENT
Silberstreifen, D-76287 Rheinstetten
Tel: +49 (0)721-51610, Fax: +49 (0)721-5161297
 

Company/Institution:

Bruker BioSpin GmbH

Name customer:

Marcel Burgers

Street:

Silberstreifen

Town:

Rheinstetten 76287

Country:

Germany

Name operator:

Mike Engelhardt

Phone (Lab):

+49 (0)721-5161-145

Fax:

+49 (0)721-5161-297

ISDN:

E-mail:

mbu@bruker.de

Spectrometer type:

AVANCE400

System order #:

HH001234

Contact Bruker BioSpin AG:

Mike Engelhardt

Phone Bruker BioSpin AG:

+49 (0)721-504-440

Fax Bruker BioSpin AG:

+49 (0)721-504-480

Email Bruker BioSpin AG:

eng@bruker.de

Email Bruker BioSpin AG:

ISDN Bruker BioSpin AG:

Sales contract #:

Service contract #:

Summary of achieved specifications
 

Result of loop over all experiments

Lineshape test for 1H with rotation

OK

Resolution test for 13C

OK

Water suppression test

OK

Dataset name: GLP.980626 1 1 v demo
 

Experiment: Lineshape test for 1H with rotation

Sample: 1% CHCl3

Specification result of humpcal:

OK

Line width at 0.55% of signal height = 7.2 Hz ( < 10Hz)

OK

Line width at 0.11% of signal height = 18.7 Hz ( < 20Hz)

OK

Half width = 0.31 Hz ( < 0.4Hz)

OK

Dataset name: GLP.980626 2 1 v demo

Experiment: Resolution test for 13C

Sample: ASTM

Specification result of hwcal:

OK

Half width = 0.08 Hz ( < 0.1Hz)

OK

Dataset name: GLP.980626 3 1 v demo

Experiment: Water suppression test

Sample: 0.002M SUCROSE

Specification result of suppcal:

OK

Line width at 50% of DDS signal = 38.3 Hz ( < 40Hz)

OK

Line width at 10% of DDS signal = 75.1 Hz ( < 80Hz)

OK

Splitting = 32 % (< 36%)

OK

Sensitivity = 86.20 :1 ( 64:1)

OK

Remarks: ____________________________________________________

Date:

Test performed by:

Test results approved by: _______________________________________

Signature: ___________________________________ Date: ___________